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The Micromeritics TriStar II Plus is a fully automated surface area and porosity analyzer that delivers a rapid high throughput analysis with high accuracy. The three-station unit increases the speed and efficiency of routine quality control analyses, yet has the accuracy, resolution, and data reduction capability to serve research requirements. The instrument combines versatility in analysis methods and data reduction to allow analyses that are customized to application needs.
Pressure Measurement | |
---|---|
Absolute | Range: 0 to 950 mmHg
Resolution: Within 0.05 mmHg Accuracy: Within 0.1% of full scale Linearity: < ± 0.1% of span |
Relative | P/Po range: 0 to 1.0 P/Po
Resolution: < 10-4-4 |
Analysis | |
Specific Surface Area | From2From 0.01 m2/g, nitrogen unit
0.001 m2krypton unit |
Total Surface Area | 0.1 m2nitrogen unit
From2From 0.001 m2/g, krypton unit |
Pore Volume | From 4 × 10-6 cm³/g |
Dewar Duration | Up to 40 hours |
Gas Consumption | Up to 300 cm³ STP per port |
Adsorptive Gases | |
Nitrogen Unit | Nitrogen; argon, carbon dioxide, or other non-corrosive gases; butane, methane, or other light hydrocarbon vapors. Oxygen can also be used only with an appropriate vacuum pump. |
Krypton Unit | Same as nitrogen unit, plus the capability to perform krypton surface area analyses at lower pressures |
The TriStar II Plus should be operated in a properly vented environment when using flammable or toxic gases. | |
Manifold Temperature | |
Transducer Accuracy | ±0.25 °C |
Resolution | Within 0.1 °C |
Vacuum System | |
Nitrogen Unit | Must accommodate 20 × 10-3 mmHg or better; uses oil-based or oil-free vacuum pump |
Krypton Unit | Must accommodate 1 × 10-3 mmHg; oil-free vacuum pump required |
Operating Environment | |
Temperature | 10 to 35 °C (50 to 95 °F), operating
0 to 50 °C (32 to 122 °F), non-operating |
Humidity | 20 to 80% relative, non-condensing |
Indoor or Outdoor Use | Indoor only
Altitude: 2000 m maximum |
Physical | |
Height | 74 cm (29 in.) |
Width | 40 cm (16 in.) |
Depth | 51 cm (20 in.) |
Weight | 37 kg (82 lbs) |
Electrical | |
Voltage | 100-240V~ |
Power | 150VA, maximum |
Frequency | 50/60Hz |
Overvoltage category | II |
Additive Manufacturing
Surface area is a critical tool in investigating the kinetics of the sintering process and product properties. Particles having rough surfaces or internal porosity will generally exhibit higher specific surface areas. Therefore, surface area indicates the amount of sample surface available to react with other component particles and/or the surrounding environment.
Adsorbents
Knowledge of surface area, total pore volume, and pore size distribution is important for quality control of industrial adsorbents and in the development of separation processes. Surface area and porosity characteristics affect the selectivity of an adsorbent.
Batteries and Fuel Cells
Optimizing the surface area and porosity of the components improves storage capacity and energy generation.
Activated Carbons
Surface area and porosity must be optimized within narrow ranges to accomplish gasoline vapor recovery in automobiles, solvent recovery in painting operations, or pollution controls in wastewater management.
Paints and Coatings
The surface area of a pigment or filler influences the gloss, texture, color, color saturation, brightness, solids content, and film adhesion properties. The porosity of a print media coating is important in offset printing where it affects blistering, ink receptivity, and ink holdout.
Pharmaceuticals
Surface area and porosity play major roles in the purification, processing, blending, tableting, and packaging of pharmaceutical products as well as their useful shelf life, dissolution rate, and bioavailability.
Catalysts
The active surface area and pore structure of catalysts influence production rates. Limiting the pore size allows only molecules of desired sizes to enter and exit, creating a selective catalyst that will produce primarily the desired product.
Ceramics
Surface area and porosity affect the curing and bonding of greenware and influence strength, texture, appearance, and density of finished goods. The surface area of glazes and glass frits affects shrinkage, crazing, and crawling. Nanotubes
Carbon Black
The wear lifetime, traction, and performance of tires are related to the surface area of carbon blacks used in their production. Medical Implants Controlling the porosity of artificial bone allows it to imitate real bone that the body will accept and allow tissue to be grown around it.
Nanotubes
Nanotube surface area and micro porosity are used to predict the capacity of a material to store hydrogen.